Sodium borohydride → HCID 67957745, compound

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Reaction Steps

To a stirred solution of product obtained in Example 3 (400 mg, 1.019 mmol) in MeOH (10 mL) was added sodium borohydride (154 mg, 4.18 mmol). The mixture was stirred at RT for 2 h and then concentrated. The resulting material was purified on silica gel eluting with 0-5% MeOH (containing 10% NH4OH)/CH2Cl2 to give the title compound as a white solid. LC/MS=365.25 [M+1].

Provenance & Evidence