HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Picolinate → Methyl 5-(4-Ethylphenyl)-6-(pyridin-4-yl)pyridine-2-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Picolinate | HCID 6920223 | — |
| Edukt | Ethyl 3-(4-Ethylphenyl)-[2,4']-bipyridinyl-6-carboxylate | HCID 68408497 | — |
| Katalysator | Sulfuric Acid | HCID 1118 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Methyl 5-(4-Ethylphenyl)-6-(pyridin-4-yl)pyridine-2-carboxylate | HCID 24752879 | — |
Reaktionsschritte
Following General Procedure E, ethyl 5-(4-ethylphenyl)-6-(pyridine-4-yl)phenyl)pyridine-2-carboxylate (Compound 49, 48 mg, 0.14 mmol) and conc. H2SO4 (10 drops) in methanol were reacted to produce the title compound as a light yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728014B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-36fda2b6e6234cea9f29b13440c68cbc |
| Quellennotiz | uspto-grants-2010_06 |