HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59382877, compound → HCID 59383036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59382877 | HCID 59382877 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 59383036 | HCID 59383036 | — |
Reaction Steps
Tert-butyl 3-(1,1,1-trifluoro-2-hydroxy-6-methoxyhexan-2-yl)piperidine-1-carboxylate (20 mg) was dissolved in 1:1 TFA/dichloromethane (4 mL). The mixture was stirred for 30 min. The mixture was concentrated to afford 1,1,1-trifluoro-6-methoxy-2-(piperidin-3-yl)hexan-2-ol which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08455521B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-2c4abd4d20094ba384ebc54b27feb14b |
| Source note | uspto-grants-2013_06 |