Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Picolinate → Methyl 5-(4-ethylphenyl)-6-(pyridin-2-yl)pyridine-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Picolinate | HCID 6920223 | — |
| 반응물 | Ethyl 3-(4-Ethylphenyl)-[2,2']-bipyridinyl-6-carboxylate | HCID 68409104 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 5-(4-ethylphenyl)-6-(pyridin-2-yl)pyridine-2-carboxylate | HCID 59338839 | — |
반응 단계
Following General Procedure E, ethyl 5-(4-ethylphenyl)-6-(pyridine-2-yl)phenyl)pyridine-2-carboxylate (Compound 50, 16 mg, 0.05 mmol) and conc. H2SO4 (10 drops) in methanol were reacted to produce the title compound as a light yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728014B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-f84eb07691ad48848f4d45b22cacaa43 |
| 출처 메모 | uspto-grants-2010_06 |