Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Quinoxaline-5-carbaldehyde → (S)-1,1-diethoxy-N-(quinoxalin-5-ylmethyl)propan-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Quinoxaline-5-carbaldehyde | HCID 582505 | — |
| 반응물 | (2S)-1,1-Diethoxy-2-propanamine | HCID 12398111 | — |
| 생성물 | (S)-1,1-diethoxy-N-(quinoxalin-5-ylmethyl)propan-2-amine | HCID 67075656 | 78.5% |
반응 단계
According to the procedure described in the synthesis method of Compound IX-2, (S)-1,1-diethoxypropan-2-amine (Compound XIX-1) 1.57 g (10.0 mmol) was reacted with quinoxaline-5-carbaldehyde 1.34 g (8.5 mmol) to obtain the title compound 1.93 g (78%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08455488B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-de67434e1e6d44a9a26689df366d6997 |
| 출처 메모 | uspto-grants-2013_06 |