huagongshe.com
HRID1255783

反应详情

EQUATION

反应方程式

HRID 1255783 的结构方程式

REACTANTS

反应物

2
结构：CNC(=S)NC(=O)OC(C)(C)C
HCID57496573

tert-Butyl (methylcarbamothioyl)carbamate

C7H14N2O2S

结构：CC[C@](N)(CC(=O)OC)c1cccc([N+](=O)[O-])c1
HCID66644170

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@]1(c2cccc([N+](=O)[O-])c2)CC(=O)N(C)C(NC(=O)OC(C)(C)C)=N1
HCID57496581

未命名化合物

PROCEDURE

实验过程

Starting from (S)-3-amino-3-(3-nitro-phenyl)-pentanoic acid methyl ester (1.2 mmole) and tert-butyl [(methylamino)carbonothioyl]carbamate, the product [(S)-4-ethyl-1-methyl-4-(3-nitro-phenyl)-6-oxo-1,4,5,6-tetrahydro-pyrimidin-2-yl]-carbamic acid tert-butyl ester (372 mg) was obtained as white solid. MS (ESI): m/z=375.4 [ M−H]−.