HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 67173096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 62506330 | HCID 62506330 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67173096 | HCID 67173096 | — |
Reaction Steps
To the solution of 2-(benzylthio)-5-nitroaniline (2.61 g, 10 mmol) in DMF (10 ml), added ethyl chloroformate (1.05 ml, 1 lmmol), followed by DIPEA (2.1 ml, 12 mmol). Stirred for 4 hours. Diluted with EtOAc, washed with water and brine, dried over Na2SO4. Concentrated to give ethyl 2-(benzylthio)-5-nitrophenylcarbamate as product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461134B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-29b558e59cf74f55939e1f3f3743e33a |
| Source note | uspto-grants-2013_06 |