HCID 59627869, compound → HCID 59627865, compound

Participants

Reaction Steps

A solution of di-tert-butyl(3-nitro-6-phenylpyridin-2-yl)imidodicarbonate (378 mg, 0.910 mmol) and MeOH (18.1 mL) was treated with 10% palladium on carbon (˜20 mg) and fitted with a hydrogen balloon. After 30 min the reaction was filtered through celite and concentrated to afford a residue which was used in the next reaction without purification. MS cal'd 386 (M+H)+, exp 386 (M+H)+.

Provenance & Evidence