HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethylaniline → 2-(4-cyanobenzyl)-N-ethyl-N'-(2-naphthylsulfonyl)-N-phenylmalonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethylaniline | HCID 7670 | — |
| Reactant | 2-(4-cyanobenzyl)-N,N-diethyl-N'-(2-naphthylsulfonyl)malonamide | HCID 86645217 | — |
| Product | 2-(4-cyanobenzyl)-N-ethyl-N'-(2-naphthylsulfonyl)-N-phenylmalonamide | HCID 68508998 | 103.9% |
Reaction Steps
In the same manner as in Example 1 (4), a crude product was obtained using the compound (300 mg) obtained in Example 111 (4) and N-ethylaniline (107 mg). This was purified by silica gel column chromatography to give the title compound (344 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461209B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-4321284db8184a3caaea9fbe2fa911f1 |
| Source note | uspto-grants-2013_06 |