2-Bromo-1-(3,4-dichlorophenyl)ethanone → HCID 58127643, compound

HRID 1257327Notes

Reaction equation

HRID 1257327 reaction equation
[NH2:1][C:2](=[S:16])[C:3]([N:6]1[CH:10]=[C:9]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:8]=[N:7]1)([CH3:5])[CH3:4].Br[CH2:18][C:19]([C:21]1[CH:26]=[CH:25][C:24]([Cl:27])=[C:23]([Cl:28])[CH:22]=1)=O>>[Cl:28][C:23]1[CH:22]=[C:21]([C:19]2[N:1]=[C:2]([C:3]([N:6]3[CH:10]=[C:9]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:8]=[N:7]3)([CH3:5])[CH3:4])[S:16][CH:18]=2)[CH:26]=[CH:25][C:24]=1[Cl:27]

Participants

3

Reactant 2

HCID 2447512-Bromo-1-(3,4-dichlorophenyl)ethanoneHCID 58127897HCID 58127897, compound

Product 1

HCID 58127643HCID 58127643, compoundYield 98%

Procedure

By a reaction in the same manner as in Example 1c and using the compound (241 mg, 1.00 mmol) obtained in Example 16b and 2-bromo-1-(3,4-dichlorophenyl)ethanone (268 mg, 1.00 mmol), the title compound (402 mg, 98%) was obtained as a colorless oil.

Workup

  1. customBy a reaction in the same manner as in Example 1c

Sources & evidence

ORD record
ord-11895042c4334e5c8094b7aaa0ac3d2d
Source dataset
uspto-grants-2013_06
Patent number
US08461348B2

Reaction notes

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