HCID 57780675, compound → HCID 86656734, compound

HRID 1257652Notes

Reaction equation

HRID 1257652 reaction equation
[CH2:1]([O:3][C:4](=N)[CH2:5][C:6]([OH:9])([CH3:8])[CH3:7])[CH3:2]>C(O)C>[CH2:1]([O:3][C:4]([O:9][CH2:6][CH3:5])([O:3][CH2:1][CH3:2])[CH2:5][C:6]([CH3:8])([OH:9])[CH3:7])[CH3:2]

Participants

3

Reactant 1

HCID 57780675HCID 57780675, compound

Product 1

HCID 86656734HCID 86656734, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 3-hydroxy-3-methyl-butyrimidic acid ethyl ester (4.40 g) in ethanol (50 mL) was left to stand for 72 hours. The mixture was filtered and the filtrate concentrated to dryness under vacuum affording 4,4,4-triethoxy-2-methyl-butan-2-ol which was used for the next step without further purification or analysis.

Workup

  1. filtrationThe mixture was filtered
  2. concentrationthe filtrate concentrated to dryness under vacuum

Sources & evidence

ORD record
ord-3a704e68d39c4f9b82b26860fc2efc75
Source dataset
uspto-grants-2013_06
Patent number
US08461328B2

Reaction notes

Loading…