HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 59354817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(4-(Quinolin-2-ylmethoxy)phenyl)acetic acid | HCID 14500235 | — |
| Product | HCID 59354817 | HCID 59354817 | 95% |
Reaction Steps
A mixture of acid 2-(4-(quinolin-2-ylmethoxy)phenyl)acetic acid (2.0 g, 6.8 mmol) in SOCl2 (10 mL) was stirred at RT for 2 h under an inert atmosphere. The reaction was concentrated in vacuo to afford 2-(4-(quinolin-2-ylmethoxy)phenyl)acetyl chloride (2.0 g, 95%) as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466148B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-719dfb26bb4d408cae83b1b8495ca99a |
| Source note | uspto-grants-2013_06 |