HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-{[(4-methylphenyl)sulfonyl]azamethylene}naphthalen-1-one → (NE)-N-[3-(1-methyltetrazol-5-yl)sulfanyl-4-oxonaphthalen-1-ylidene]-4-phenylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-{[(4-methylphenyl)sulfonyl]azamethylene}naphthalen-1-one | HCID 5717988 | — |
| Reactant | (NE)-N-[3-(1-methyltetrazol-5-yl)sulfanyl-4-oxonaphthalen-1-ylidene]-4-phenylbenzenesulfonamide | HCID 46908285 | — |
| Reactant | HCID 178527894 | HCID 178527894 | — |
| Product | (NE)-N-[3-(1-methyltetrazol-5-yl)sulfanyl-4-oxonaphthalen-1-ylidene]-4-phenylbenzenesulfonamide | HCID 46908285 | 70.2% |
| Product | HCID 178427421 | HCID 178427421 | — |
Reaction Steps
(E)-N-(3-(1H-1,2,4-triazol-3-ylthio)-4-oxonaphthalen-1(4H)-ylidene)-4-methylbenzenesulfonamide (13k) was prepared according to the procedure for 13x except using 12i and 3-mercapto-1,2,4-triazole, affording 57.6 mg (70.2%) title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466157B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-c215bda457db4c47a802ab4521866ad9 |
| Source note | uspto-grants-2013_06 |