HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 66584337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178526400 | HCID 178526400 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 66584337 | HCID 66584337 | 345.9% |
Reaction Steps
Compounds 6 (3 g, 13.18 mmole) and 17 (3.9 g, 13.18 mmole) were combined in CH3CN (25 mL) and heated for one hr. Mass spectroscopy indicated no starting material. Saturated K2CO3 was added and the reaction was extracted 3× with EtOAc. The organic layers were combined, washed with brine and concentrated in vacuo to give 6.48 g of 7 (78.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466165B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-dbfc1af4d5144f629cb1e324fdc3abe3 |
| Source note | uspto-grants-2013_06 |