Triethylamine → HCID 57551982, compound

Participants

Reaction Steps

To a stirred solution of compound 12d (500 mg, 1.55 mmol) in CH2Cl2 (20 mL) was added triethyl amine (332 μL, 2.32 mmol) and mesyl chloride (266 mg, 2.32 mmol). After stirring for 30 minutes the reaction was washed with saturated NaHCO3 (1×20 mL), 2M HCl (1×20 m), dried MgSO4 and concentrated to give the title compound (655 mg, 99%) as a yellow oil. MS M+H 402.

Provenance & Evidence