HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-Acetylamino-N-methoxy-N-methyl-5-(pentafluorosulfanyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Trifluoroacetic anhydride | HCID 9845 | — |
| Reactant | 3-Amino-N-methoxy-N-methyl-5-pentafluorosulfanylbenzamide | HCID 58085703 | — |
| Product | 3-Acetylamino-N-methoxy-N-methyl-5-(pentafluorosulfanyl)benzamide | HCID 58136820 | — |
Reaction Steps
3-Amino-N-methoxy-N-methyl-5-pentafluorosulfanylbenzamide (1.2 g, example 4b) was reacted analogously to example 4c) with acetic anhydride instead of with trifluoroacetic anhydride. 1.3 g of the desired compound were isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466169B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-fe519ad68b624a78b9139597ce1becb2 |
| Source note | uspto-grants-2013_06 |