Methanamine, N-methoxy-, hydrochloride (1:1) → HCID 58137433, compound

HRID 1258512Notes

Reaction equation

HRID 1258512 reaction equation
[NH2:1][C:2]1[CH:10]=[C:9]([S:11]([F:16])([F:15])([F:14])([F:13])[F:12])[CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].Cl.[CH3:18][NH:19][O:20][CH3:21]>>[NH2:1][C:2]1[CH:10]=[C:9]([S:11]([F:16])([F:15])([F:14])([F:13])[F:12])[CH:8]=[CH:7][C:3]=1[C:4]([N:19]([O:20][CH3:21])[CH3:18])=[O:5]

Participants

3

Reactant 2

HCID 81138Methanamine, N-methoxy-, hydrochloride (1:1)HCID 58137424HCID 58137424, compound

Product 1

HCID 58137433HCID 58137433, compound

Procedure

2-Amino-4-(pentafluorosulfanyl)benzoic acid (2.0 g) was reacted with N,O-dimethylhydroxylamine hydrochloride analogously to example 15a). 2.3 g of the desired product were obtained.

Sources & evidence

ORD record
ord-e620f3961a0b4ed5a273c6f5b4f0a29b
Source dataset
uspto-grants-2013_06
Patent number
US08466169B2

Reaction notes

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