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Potassium Carbonate → 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-(Trifluoromethyl)piperidine | HCID 136469 | — |
| 反応物 | 4,5-Dichloro-n-methyl-2-nitroaniline | HCID 289317 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline | HCID 44120655 | — |
反応手順
The sub-title compound was prepared from 4,5-dichloro-2-nitro-N-methyl-aniline (820 mg, 3.7 mmol), 4-trifluoromethyl-piperidine (680 mg, 4.5 mmol) and potassium carbonate (770 mg, 5.6 mmol) in DMSO (10 mL) in analogy to example 3, step (a).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08466186B2 |
| 出典データセット | uspto-grants-2013_06 |
| ORD ID | ord-9240ae367e324c91b9e6d9ef1785bbb1 |
| 出典メモ | uspto-grants-2013_06 |