Stannous chloride dihydrate → HCID 67957795, compound

Participants

Reaction Steps

Tin dichloride dihydrate (710 mg, 3.1 mmol) was added to 4-chloro-5-(2-dimethylcarbamoyl-pyrrolidin-1-yl)-2-nitroaniline (200 mg, 0.6 mmol) in EtOAc (5 mL). The reaction mixture was stirred at reflux for 3 h, cooled and poured into sat.aq. NaHCO3-solution. The mixture was filtered through a pad of celite. The organic layer was dried over Na2SO4 and concentrated to give the sub-title compound.

Provenance & Evidence