HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylbenzylamine → N-(2-Methoxyethyl)-N-methylbenzenemethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylbenzylamine | HCID 7669 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(2-Methoxyethyl)-N-methylbenzenemethanamine | HCID 21843648 | 58% |
Reaction Steps
The synthesis of BnMO was carried out in a manner similar to that of BnEO (process 2) using N-methylbenzylamine (15 mL, 0.116 mol), bromoethyl methyl ether (12 mL, 0.116×1.1 mmol), and ethanol (200 mL) as a solvent. BnMO (12.09 g, 67.46 mmol, yield 58%) was obtained as a pale yellow clear liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466287B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-b3d702dd81b64101bc4909d8858fe53e |
| Source note | uspto-grants-2013_06 |