Chlorosuccinimide → HCID 178453614, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 1C (336 mg, 0.6 mmol) and NCS (104 mg, 0.78 mmol) in chloroform (20 mL) was stirred at 60° C. under N2. After 1.5 h, the mixture was cooled to rt and concentrated. Reverse-phase HPLC purification gave ID as a light yellow solid. LC/MS m/z 596.2 (M+H)+.

Provenance & Evidence