HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 67320757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 58355139 | HCID 58355139 | — |
| Product | HCID 67320757 | HCID 67320757 | — |
Reaction Steps
tert-Butyl (3S,5R)-3-[{[1-(2-fluorophenyl)-5-(4-methoxybutyl)-1H-1,2,3-triazol-4-yl]carbonyl}(2-methylpropyl)amino]-5-(hydroxymethyl)piperidine-1-carboxylate (400 mg) was dissolved in 10% hydrogen chloride-methanol (4 ml), and the mixture was stirred at room temperature for 18 hr. The reaction mixture was concentrated to give the object product (334 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466282B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-48497d1c8f564e0f8c03e4603d61f1b6 |
| Source note | uspto-grants-2013_06 |