Aniline → HCID 20502989, compound

HRID 1260408Notes

Reaction equation

HRID 1260408 reaction equation
NC1N=C(N[C@H:9]2[CH2:13][C@@H:12]([CH2:14][OH:15])[C@H:11]([OH:16])[C@@H:10]2[OH:17])C(N=NC2C=CC(Cl)=CC=2)=C(Cl)N=1.NC1C=CC=CC=1>>[OH:15][CH2:14][CH:12]1[CH:11]([OH:16])[CH:10]([OH:17])[CH2:9][CH2:13]1

Participants

3

Reactant 2

HCID 6115AnilineHCID 46178398HCID 46178398, compound

Product 1

HCID 20502989HCID 20502989, compound

Procedure

Compound 1, (1S,2R,3S,5S)-3-[[2-amino-6-chloro-5-phenylazo]-4-pyrimidinyl]amino]-5-(hydroxymethyl)-1,2-cyclopentanediol was prepared by the same method used for Compound 11, using a stoichiometric amount of aniline instead of 4-chloroaniline.

Sources & evidence

ORD record
ord-8acaa4791d824e59b807e8bef650a2ff
Source dataset
uspto-grants-2013_06
Patent number
US08470834B2

Reaction notes

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