N-(4,4-diethoxybutyl)acetamide → HCID 44608466, compound

HRID 1260511Notes

Reaction equation

HRID 1260511 reaction equation
[CH:1]1([O:6][C:7]2[CH:18]=[CH:17][C:10]([CH2:11][CH:12]([CH2:15][OH:16])[CH2:13][OH:14])=[CH:9][CH:8]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.C(O[CH:22](OCC)[CH2:23][CH2:24][CH2:25][NH:26][C:27](=[O:29])[CH3:28])C>>[CH:1]1([O:6][C:7]2[CH:18]=[CH:17][C:10]([CH2:11][CH:12]3[CH2:13][O:14][CH:22]([CH2:23][CH2:24][CH2:25][NH:26][C:27](=[O:29])[CH3:28])[O:16][CH2:15]3)=[CH:9][CH:8]=2)[CH2:2][CH2:3][CH2:4][CH2:5]1

Participants

3

Reactant 2

HCID 12677171N-(4,4-diethoxybutyl)acetamideHCID 67071558HCID 67071558, compound

Product 1

HCID 44608466HCID 44608466, compound

Procedure

2-(4-Cyclopentyloxybenzyl)propane-1,3-diol (92 mg, 337 μmol) was reacted with N-(4,4-diethoxybutyl)acetamide in analogy to example 3d. Yield: 81 mg (60%), M+H+: 362.27.

Sources & evidence

ORD record
ord-0add20d66d994fc49d853787796a3dc1
Source dataset
uspto-grants-2013_06
Patent number
US08470841B2

Reaction notes

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