HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4,4-diethoxybutyl)acetamide → HCID 44608787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4,4-diethoxybutyl)acetamide | HCID 12677171 | — |
| Reactant | HCID 49855595 | HCID 49855595 | — |
| Reactant | HCID 178474772 | HCID 178474772 | — |
| Reactant | HCID 178474773 | HCID 178474773 | — |
| Product | HCID 44608787 | HCID 44608787 | — |
Reaction Steps
2-(5-Benzyloxypyridin-2-yloxy)propane-1,3-diol (216 mg, 784 μmol) was reacted with N-(4,4-diethoxybutyl)acetamide in analogy to example 3d. Yield: cis-N-{3-[5-(5-benzyloxypyridin-2-yloxy)-[1,3]dioxan-2-yl]propyl}acetamide (example 16), 21 mg (7%), M+H+: 387.22 and trans-N-{3-[5-(5-benzyloxypyridin-2-yloxy)-[1,3]dioxan-2-yl]propyl}acetamide (example 17), 6 mg (2%), M+H+: 387.23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-fba0632726a74c869ffa51cc0c5cd7cb |
| Source note | uspto-grants-2013_06 |