Acetic Anhydride → HCID 67071697, compound

HRID 1260530Notes

Reaction equation

[NH2:1][C@@H:2]([CH3:12])[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1.[C:13](OC(=O)C)(=[O:15])[CH3:14]>>[OH:11][C:8]1[CH:7]=[CH:6][C:5]([CH2:4][CH2:3][C@@H:2]([NH:1][C:13](=[O:15])[CH3:14])[CH3:12])=[CH:10][CH:9]=1

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 228315064-(3-Aminobutyl)phenol, (S)-

Product 1

HCID 67071697HCID 67071697, compound

Procedure

4-((S)-3-Aminobutyl)phenol (1.3 g, 7.87 mmol) was reacted with acetic anhydride in analogy to example 2a. Yield: 1.24 g (76%), M+H+: 208.13.

Sources & evidence

ORD record: ord-ad8bea075af2411686a3aeee9728e1e3
Source dataset: uspto-grants-2013_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08470841B2

Reaction notes

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