HRID1260763

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID350846

Methyl 4,4-dimethoxybutyrate

C7H14O4

结构：Cl.Cl.Cl.N[C@H]1CC[C@H](CCN2CCN(c3nccc4c3OCC4)CC2)CC1

HCID178478590

未命名化合物

2 次

PRODUCTS

生成物

结构：COC(CCC(=O)N[C@H]1CC[C@H](CCN2CCN(c3nccc4c3OCC4)CC2)CC1)OC

HCID178495093

未命名化合物

PROCEDURE

实验过程

The title compound, white solid (110 mg, 96%), MS (ISP) m/z=461.4 [(M+H)+], mp 204.5° C., was prepared in accordance with the general method of example 5 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and methyl 4,4-dimethoxy-butanoate.