HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridin-3-yl-benzoic acid → HCID 178523724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridin-3-yl-benzoic acid | HCID 1515244 | — |
| Reactant | HCID 178478590 | HCID 178478590 | — |
| Product | HCID 178523724 | HCID 178523724 | — |
Reaction Steps
The title compound, white solid (109 mg, 85%), MS (ISP) m/z=512.6 [(M+H)+], mp 235° C., was prepared in accordance with the general method of example 6 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and 4-(pyridin-3-yl)-benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470828B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-2485be4d118a452b8c8faaf44c98c7da |
| Source note | uspto-grants-2013_06 |