HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methanesulfonylthiophene-2-carboxylic acid → HCID 178504776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methanesulfonylthiophene-2-carboxylic acid | HCID 2740497 | — |
| Reactant | HCID 178478590 | HCID 178478590 | — |
| Product | HCID 178504776 | HCID 178504776 | — |
Reaction Steps
The title compound, white solid (120 mg, 93%), MS (ISP) m/z=519.3 [(M+H)+], mp 212° C., was prepared in accordance with the general method of example 6 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and 5-methanesulfonyl-thiophene-2-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470828B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-859bb81d79d24b23affb8db194225980 |
| Source note | uspto-grants-2013_06 |