HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 59596843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 59596825 | HCID 59596825 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 59596843 | HCID 59596843 | — |
Reaction Steps
A mixture of 2.68 g (12.8 mmol) of 1-fluoro-4-methyl-2-(2,2,2-trifluoro-ethoxy)-benzene, 2.3 g (12.9 mmol) of NBS and 140 mg of dibenzoylperoxide in 60 ml of CCl4 was refluxed for 6 hours. Solvent was removed and the crude residue was used without any further purification for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470877B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-0e01217f33764af5802fcf26f4bda39f |
| Source note | uspto-grants-2013_06 |