反应详情

温度

90 °C

1,5-Di(tert-butyl)-1,1,3,5,5-Pentamethyltrisiloxane and Karstedt's catalyst (30 ppm) were charged to a 100 mL Schlenk flask. The mixture was heated to 90° C. and N,N-dimethyl allyl amine (4.48 g) was added dropwise via syringe over 5 minutes. After complete addition, the reaction temperature was maintained at 90° C. for 3 hrs and the reaction was monitored by 1HNMR spectroscopy. Upon reaction completion, the volatiles were removed at 100° C./0.1 mmHg, and 15.2 g light yellow oil product was obtained.

1. additionAfter complete addition
2. temperaturethe reaction temperature was maintained at 90° C. for 3 hrs
3. customUpon reaction completion
4. customthe volatiles were removed at 100° C./0.1 mmHg, and 15.2 g light yellow oil product
5. customwas obtained