HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 75058736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 75058734 | HCID 75058734 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 75058736 | HCID 75058736 | — |
Reaction Steps
After dissolving Compound A, which was obtained in Synthesis Example 1, in methanol, the anion thereof was replaced with methanesulfonic acid according to an ordinary method to give 2-((3-ethyl-5-(2-(3-methylbenzo[d]thiazol-2(3H)-ylidene)ethylidene)-4-oxothiazolidin-2-ylidene)methyl)-5-fluoro-3-methylbenzo[d]thiazol-3-ium mesylate (Compound D) as a dark-green solid. The physical property values and analytical values of this compound are as described below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08471036B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-2ccc91a48ba6404693bda47097a04bfc |
| Source note | uspto-grants-2013_06 |