HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(2-Morpholin-4-ylethoxy)aniline → HCID 66712107, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(2-Morpholin-4-ylethoxy)aniline | HCID 6486616 | — |
| Edukt | N-[2-(2-methylsulfinyl-pyrrolo[2,1-f][1,2,4]triazin-7-yl)-phenyl]-methanesulfonamide | HCID 66711409 | — |
| Produkt | HCID 66712107 | HCID 66712107 | — |
Reaktionsschritte
Prepared by following a procedure analagous to Example 251c by using 3-(2-Morpholin-4-yl-ethoxy)-phenylamine and N-[2-(2-Methanesulfinyl-pyrrolo[2,1-f][1,2,4]triazin-7-yl)-phenyl]-methanesulfonamide. 1H-NMR (DMSO) δ 9.9 (br s, 1H), 9.6 (s, 1H), 9 (s, 1H), 8.8 (s, 1H), 7.7 (d, J=8.0 Hz, 1H), 7.6 (m, 2H), 7.5 (m, 1H), 7.4 (brs, 1H), 7.2 (m, 1H), 7.1 (t, J=8.0 Hz, 1H), 7 (s, 2H), 6.6 (d, J=7.2 Hz, 1H), 4.1-3 (m, 12H), 2.7 (s, 3H); LC/MS (ESI+): 509 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08471005B2 |
| Quelldatensatz | uspto-grants-2013_06 |
| ORD ID | ord-c0344c241ee7460289c7aed379e1209b |
| Quellennotiz | uspto-grants-2013_06 |