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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1262539Generated: October 30, 2026

Triethylamine → HCID 86739455, compound

https://huagongshe.com/reaction/1262539

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantGlycine methyl ester hydrochlorideHCID 122755—
ReactantHCID 86739456HCID 86739456—
SolventChloroformHCID 6212—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86739455HCID 86739455—

Reaction Steps

4-Allyloxy-3-chloro-phenylacetyl-(DL)-phenylalanyl-(DL)-phenylalanine (1.20 g) was dissolved in dry tetrahydrofuran (10 ml). To the solution was added glycine methyl ester hydrochloride (0.25 g) in dry chloroform (10 ml) containing dry triethylamine (0.28 ml). DCC (0.41 g) was added and the reaction mixture was stirred overnight at room temperature. DCU was then filtered off.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04452783
Source datasetuspto-grants-1984_06
ORD IDord-d77177516d144ea68555263e7633a35a
Source noteuspto-grants-1984_06