HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13320263, compound → HCID 13192218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13320263 | HCID 13320263 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13192218 | HCID 13192218 | — |
Reaction Steps
Eighteen grams of 1-benzyl-4-(1-naphthoxy)-3-pyrrolidinol in 200 ml. of ethanol was treated with ca. 2 g. of 10% palladium-on-charcoal under hydrogen at 60° C. for 20 hr. The mixture was cooled, filtered and ethanol removed. The residue was crystallized from benzene and had a melting point of 112°-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04452809 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-71a622556c1043008fa0672992d5e2a9 |
| Source note | uspto-grants-1984_06 |