HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13320299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 70454232 | HCID 70454232 | — |
| Product | HCID 13320299 | HCID 13320299 | — |
Reaction Steps
A mixture of 15.2 g. (0.05 mole) of cis-4-(3-chlorophenoxy)-1-phenylmethyl-3-pyrrolidinol and 56 g. (0.4 mole) of methyl iodide was heated at reflux for 60 hr. Excess methyl iodide was removed under vacuum. The pasty residue was washed with ether-acetone, leaving 13 g. (59%) of granular tan powder, m.p. 118-25° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04452809 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-f9c1dfc0bc83402e88495ab477c0fdf1 |
| Source note | uspto-grants-1984_06 |