HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → 3-(Trimethylsilyloxy)-1-butyne
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | 3-Butyn-2-ol | HCID 16239 | — |
| Product | 3-(Trimethylsilyloxy)-1-butyne | HCID 28817 | 60% |
Reaction Steps
The above compound was prepared in a 60 % yield from 35 g of but-3-yn-2-ol and 50.4 g of trimethylsilyl chloride according to the method given in Can. J. Chem. 43, 2004 (1965); b.p. 117°/760 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04453013 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-065a5396889840faad71e7543b56663e |
| Source note | uspto-grants-1984_06 |