HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 13072168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 8-Quinolinesulfonamide | HCID 94464 | — |
| Reactant | 2,4-Dichloro-6-isocyanato-1,3,5-triazine | HCID 13052624 | — |
| Product | HCID 13072168 | HCID 13072168 | — |
Reaction Steps
To a stirred mixture of 1.8 g of 8-quinolinesulfonamide in 15 ml tetrahydrofuran is added 2.3 g of 2-isocyanato-4,6-dichloro-1,3,5-triazine. This mixture is then heated to reflux temperature for 21/2 hours, then cooled to room temperature, filtered and the resultant filtrate triturated with hexanes and filtered to give 1.8 g solid, m.p. 198°-200°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04453970 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-d8c214815d3f4ee9974d4a132fa962ce |
| Source note | uspto-grants-1984_06 |