3-Pyridinecarbonyl chloride, hydrochloride (1:1) → 2,2,11,11-Tetramethyldodecane-1,12-diyl dipyridine-3-carboxylate

Participants

Reaction Steps

53.10 Grams (0.3 mole) of nicotinoyl chloride hydrochloride in 150 ml of anhydrous pyridine were reacted with 12.90 grams (0.05 mole) of 2,2,11,11-tetramethyl-1,12-dodecanediol according to the procedure of the above example. 11.8 Grams of the title product, recrystallized from an 80/20 (v/v) mixture of ethanol/water, were obtained, having m.p. 66°-67° C. Yield: 50.5% of theoretical.

Provenance & Evidence