HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13320134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 13320091 | HCID 13320091 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13320134 | HCID 13320134 | — |
Reaction Steps
Treatment of 1,1-dibromo-2-phenyl-3-phthalimidopropene (421 mg) with hydrazine hydrate (55 mg) and methanol (6 ml) followed by 50% aqueous hydrochloric acid as described in Example 19 D gives 2-phenyl-3,3-dibromoallylamine hydrochloride (175 mg): colorless needles; m.p. 243°-244°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04454158 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-7622e9a37c4b4392b852ea3942e20dfd |
| Source note | uspto-grants-1984_06 |