HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 22826725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 86739481 | HCID 86739481 | — |
| Solvent | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 22826725 | HCID 22826725 | 112.3% |
Reaction Steps
A solution of N2 -(tert-butyloxycarbonyl)-N-methyl-N-(3-phenylpropyl)-D-methioninamide (4.06 g.) in hydrogen chloride-ethyl acetate (3.9 N, 20 ml.) was stirred at room temperature for 40 minutes. Ether (100 ml.) was added, precipitating an oil, and the mixture was stripped of volatiles under vacuum, affording N-methyl-N-(3-phenylpropyl)-D-methioninamide (3.13 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04454120 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-95c56d7b59ab41518134fd48764d8292 |
| Source note | uspto-grants-1984_06 |