Trichlorosilane → HCID 57207834, compound

HRID 1262948Notes

Reaction equation

HRID 1262948 reaction equation
[F:1][CH:2]([O:7][CH2:8][CH:9]=[CH2:10])[C:3]([F:6])([F:5])[F:4].[Cl:11][SiH:12]([Cl:14])[Cl:13]>C(Cl)(Cl)Cl>[F:1][CH:2]([O:7][CH2:8][CH2:9][CH2:10][Si:12]([Cl:14])([Cl:13])[Cl:11])[C:3]([F:6])([F:5])[F:4]

Participants

4

Reactant 2

HCID 24811TrichlorosilaneHCID 14597123HCID 14597123, compound

Product 1

HCID 57207834HCID 57207834, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Each hour, 1.5 liters (11.3 moles) of tetrafluoroethylallylether, 1.3 liters (12.7 moles) trichlorosilane and 10 ml of a catalyst solution are added to the reactor. The catalyst solution is prepared by dissolving 19.4 g of tetrachlorodioctenediplatinum (II) in 1000 ml of chloroform.

Workup

  1. customThe catalyst solution is prepared

Sources & evidence

ORD record
ord-87e1977214264fe3b53f3822d79a6920
Source dataset
uspto-grants-1984_06
Patent number
US04454331

Reaction notes

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