化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → (2-Nitrophenyl)methanesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | (2-nitrophenyl)methanesulfonyl Chloride | HCID 4305447 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | (2-Nitrophenyl)methanesulfonamide | HCID 13266249 | — |
反応手順
To a suspension of 29.4 g of the product of Example 2 in 250 ml of diethyl ether was added 6.5 ml of anhydrous ammonia at 5°-15°. After stirring at 15°-25° for 1 hour, the product was filtered off, washed with ether, and water and oven dried at 60° to give 20.5 g of 2-nitrophenylmethanesulfonamide, m.p.=134°-136°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04454334 |
| 出典データセット | uspto-grants-1984_06 |
| ORD ID | ord-3fa59f30c0f64aa8a28a7b4164f4875c |
| 出典メモ | uspto-grants-1984_06 |