Phenol → Magnesium di(phenolate)

HRID 1263014Notes

Reaction equation

HRID 1263014 reaction equation
[O-2].[Mg+2:2].[C:3]1([OH:9])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>>[C:3]1([O-:9])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[Mg+2:2].[C:3]1([O-:9])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 996PhenolHCID 6850729Magnesium monoxide

Product 1

HCID 13616137Magnesium di(phenolate)

Procedure

A powder of commercial magnesium oxide (80 g) calcined at 550° C. and 282 g of phenol were charged in a ball mill and mixed at 150° C. for 16 hours. Phenol was thoroughly removed by vacuum evaporation to give magnesium phenolate-containing magnesium oxide of particle sizes 10-16 mesh.

Workup

  1. customcalcined at 550° C.
  2. additionmixed at 150° C. for 16 hours
  3. customPhenol was thoroughly removed by vacuum evaporation

Sources & evidence

ORD record
ord-e697ccd974f649f2a39960cb12aebbb8
Source dataset
uspto-grants-1984_06
Patent number
US04454357

Reaction notes

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