HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → Magnesium di(phenolate)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Methanol, magnesium salt (2:1) | HCID 164537 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | Magnesium di(phenolate) | HCID 13616137 | 93.7% |
Reaction Steps
A mixture of 48.5 g of this magnesium methylate and 105 g of phenol was suspended in 150 ml of n-heptane. The suspension was heated to reflux n-heptane at 98° C. for 10 hours, then cooled, and evaporated in a rotary evaporator to remove n-heptane and methanol, thereby giving 110 g of magnesium phenolate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04454357 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-7c502f39682245b0b171491ae60b2f62 |
| Source note | uspto-grants-1984_06 |