HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13343566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13343565 | HCID 13343565 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13343566 | HCID 13343566 | — |
Reaction Steps
To dimethyl 2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenoxymethylphosphonate (0.5 g) in benzene (10 ml) is added thionyl chloride (8 ml) at RT. The mixture is allowed to return to RT and is stirred for 6 hours. The solvent and any excess thionyl chloride are then distilled off, yielding methyl 2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenoxymethylphosphonochloridate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04456464 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-60d91b45cbaa431188769cb3048e1bc5 |
| Source note | uspto-grants-1984_06 |