HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylmaleimide → HCID 13547657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylmaleimide | HCID 70261 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13547657 | HCID 13547657 | 88% |
Reaction Steps
The procedure of Example 1 is repeated using 11.92 grams 2,6-di-tert-butyl-4-mercaptophenol, 5.55 grams N-methylmaleimide, and 0.5 grams triethylamine. The residue is recrystallized from toluene: heptane to give 15.47 grams (88% yield), m.p. 132°-132.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04456716 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-d0bb040fe07a4923907dd66a3780f2b2 |
| Source note | uspto-grants-1984_06 |