HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-mercaptophenol → HCID 13547658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | 1-Butyl-1H-pyrrole-2,5-dione | HCID 239780 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13547658 | HCID 13547658 | — |
Reaction Steps
The procedure of Example 1 is repeated using 11.92 grams 2,6-di-tert-butyl-4-mercaptophenol, 7.66 grams N-n-butylmaleimide, and 0.5 grams triethylamine. The residue is purified by dry column chromatography to give a white solid, m.p. 80°-85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04456716 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-dedc98bbc7ed48c6843234c5475769f7 |
| Source note | uspto-grants-1984_06 |