HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1263401Generated: November 1, 2026
Methanol → Methyl 3-amino-2-methyl-4-methylsulfanylbenzoate
https://huagongshe.com/reaction/1263401
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Amino-2-methyl-4-methylsulfanylbenzoic acid | HCID 18616043 | — |
| Product | Methyl 3-amino-2-methyl-4-methylsulfanylbenzoate | HCID 18616042 | — |
Reaction Steps
2 g of 3-amino-2-methyl-4-methylsulfanylbenzoic acid (0.01 mol) were dissolved in 20 ml of methanol and admixed with 2.0 g of conc. sulfuric acid, and the mixture was heated at 60° C. for 2 h. After cooling, the reaction mixture was poured into water, neutralized and extracted with ethyl acetate. After washing and drying, the solvent was removed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06541423B1 |
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| Source dataset | uspto-grants-2003_04 |
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| ORD ID | ord-adc3aed3da0748789b8aeddf54f0e51c |
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| Source note | uspto-grants-2003_04 |
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