HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-methyl-3-nitrobenzoate → 3-Amino-2-methylbenzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-methyl-3-nitrobenzoate | HCID 601165 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-2-methylbenzoic acid methyl ester | HCID 3801025 | — |
Reaction Steps
210 g of methyl 2-methyl-3-nitrobenzoate (1.08 mol) were dissolved in 4 l of methanol, 21 g of Pd/C were added and the mixture was subsequently hydrogenated at ambient pressure. After the reaction had ended, the catalyst was filtered off and the solvent was removed. Yield: 178 g (quant.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541423B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-2446028f7ca14a37a4b8d6af37e2a55f |
| Source note | uspto-grants-2003_04 |